Table 3: Calibration solutions [CS] of PCDD/PCDF (ng/ml).
Analyte |
Caibration levels |
||||||||
Native standard |
CS1 |
CS2 |
CS3 |
CS4 |
CS5 |
CS6 |
CS7 |
CS8 |
CS9 |
2,3,7,8 - TCDD |
0.025 |
0.05 |
0.1 |
0.5 |
2 |
5 |
10 |
20 |
50 |
2,3,7,8-ТCDF |
0.025 |
0.05 |
0.1 |
0.5 |
2 |
5 |
10 |
20 |
50 |
1,2,3,7,8-PCDD |
0.025 |
0.05 |
0.1 |
0.5 |
2 |
5 |
10 |
20 |
50 |
1,2,3,7,8-PCDF |
0.025 |
0.05 |
0.1 |
0.5 |
2 |
5 |
10 |
20 |
50 |
2,3,4,7,8-PCDF |
0.025 |
0.05 |
0.1 |
0.5 |
2 |
5 |
10 |
20 |
50 |
1,2,3,4,7,8-HXDF |
0.05 |
0.1 |
0.2 |
1 |
4 |
10 |
20 |
40 |
100 |
1,2,3,6,7,8-HXDF |
0.05 |
0.1 |
0.2 |
1 |
4 |
10 |
20 |
40 |
100 |
2,3,4,6,7,8-HXDF |
0.05 |
0.1 |
0.2 |
1 |
4 |
10 |
20 |
40 |
100 |
1,2,3,4,7,8-HXDD |
0.05 |
0.1 |
0.2 |
1 |
4 |
10 |
20 |
40 |
100 |
1,2,3,6,7,8-HXDD |
0.05 |
0.1 |
0.2 |
1 |
4 |
10 |
20 |
40 |
100 |
1,2,3,7,8,9-HXDD |
0.05 |
0.1 |
0.2 |
1 |
4 |
10 |
20 |
40 |
100 |
1,2,3,7,8,9-HXDF |
0.05 |
0.1 |
0.2 |
1 |
4 |
10 |
20 |
40 |
100 |
1,2,3,4,6,7,8-HPDF |
0.05 |
0.1 |
0.2 |
1 |
4 |
10 |
20 |
40 |
100 |
1,2,3,4,6,7,8-HPDD |
0.05 |
0.1 |
0.2 |
1 |
4 |
10 |
20 |
40 |
100 |
1,2,3,4,7,8,9-HPDF |
0.05 |
0.1 |
0.2 |
1 |
4 |
10 |
20 |
40 |
100 |
OCDD |
0.1 |
0.2 |
0.4 |
2 |
8 |
20 |
40 |
80 |
200 |
OCDF |
0.1 |
0.2 |
0.4 |
2 |
8 |
20 |
40 |
80 |
200 |
Internal standards |
|||||||||
13С12 - 2,3,7,8 - TCDD |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
13С12 - 2,3,7,8-ТCDF |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
13С12 - 1,2,3,7,8-PCDD |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
13С12 - 1,2,3,7,8-PCDF |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
13С12 - 2,3,4,7,8-PCDF |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
13С12 - 1,2,3,4,7,8-HXDF |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
13С12 - 1,2,3,6,7,8-HXDF |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
13С12 - 2,3,4,6,7,8-HXDF |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
13С12 - 1,2,3,4,7,8-HXDD |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
13С12 - 1,2,3,6,7,8-HXDD |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
13С12 - 1,2,3,7,8,9-HXDD |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
13С12 - 1,2,3,7,8,9-HXDF |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
13С12 - 1,2,3,4,6,7,8-HPDF |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
13С12 - 1,2,3,4,6,7,8-HPDD |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
13С12 - 1,2,3,4,7,8,9-HPDF |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
13С12 - OCDD |
4 |
4 |
4 |
4 |
4 |
4 |
4 |
4 |
4 |
13С12 - OCDF |
4 |
4 |
4 |
4 |
4 |
4 |
4 |
4 |
4 |
Recovery standards |
|||||||||
13С12 - 1,2,3,4 - TCDD |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
13С12 -12,3,4,6,9 - HXDF |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
13С12 -1,2,3,4,6,8,9 - HPDF |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |
2 |